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Google Patents Electrically non-conductive, nanoparticulate membraneĭownload PDF Info Publication number US7563588B2 US7563588B2 US10/577,292 US57729204A US7563588B2 US 7563588 B2 US7563588 B2 US 7563588B2 US 57729204 A US57729204 A US 57729204A US 7563588 B2 US7563588 B2 US 7563588B2 Authority US United States Prior art keywords membrane oxidase redox glucose dehydrogenase Prior art date Legal status (The legal status is an assumption and is not a legal conclusion. Google Patents US7563588B2 - Electrically non-conductive, nanoparticulate membrane The results indicate that the modification of graphite‐composite electrodes with Bi2O3 nanostructures improved analytical characteristics of electrochemical sensors for trace‐metal determinations.US7563588B2 - Electrically non-conductive, nanoparticulate membrane Graphite‐composite electrodes bulk‐modified with Bi2O3 nanostructures provided higher sensitivity and lower detection limits for determinations of cadmium, lead and zinc (0.26 0.52 and 2.23 µg L−1, respectively) employing short deposition time (60 s). The bismuth nanostructures were produced under microwave‐hydrothermal conditions followed by thermal conversion of as‐prepared precursor and characterized by X‐ray diffraction, Fourier‐transformed infrared and field‐emission scanning‐electron‐microscopy. We describe the preparation of bismutite ((BiO)2CO3) and bismuth‐oxide (Bi2O3) plates‐like nanostructures and their incorporation within graphite‐composite electrodes for the determination of trace metals by anodic‐stripping‐voltammetry. CV experiments were performed at 100 ☌ for pure IL (purged Zn2þ þ 2O 2 ZnO4 ZnO2 þ O2 ZnO þ 32O2 ð3Þ by Ar flow), each independent precursor (O2 and Zn(TFSI)2) solu- tion and for the full.
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Graphite‐Composite Electrodes Bulk‐Modified with (BiO) 2 CO 3 and Bi 2 O 3 Plates‐Like Nanostructures for Trace Metal Determination by Anodic Stripping Voltammetry Graphite‐Composite Electrodes Bulk‐Modified with (BiO) 2 CO 3 and Bi 2 O 3 Plates‐Like. carried Zn2þ þ 2e Zn ð2Þ out using an Autolab PGSTAT302N and GPES software (Eco Chemie B.V.).